By Frank Parker
This e-book isn't really meant to be a easy textual content in infrared spectroscopy. Many such books exist and i've spoke of them within the textual content. fairly, i've got attempted to discover functions that may be fascinating to various humans: complex undergraduate chemistry scholars, graduate scholars and learn employees in numerous disciplines, spectros copists, and physicians energetic in examine or within the perform of drugs. With this target in brain there has been no purpose to have exhaustive assurance of the literature. I should still wish to recognize my use of numerous books and reports, which have been valuable in my look for fabric: G. H. Beaven, E. A. Johnson, H. A. Willis and R. G. 1. Miller, Molecular Spec troscopy, Heywood and corporate, Ltd., London, 1961. J. A. Schell guy and Charlotte Schellman, 'The Conformation of Polypeptide Chains in Proteins," within the Proteins, Vol. II, 2d Ed. (H. Neurath, ed.), educational Press, long island, 1964. R. T. O'Connor, "Application of Infrared Spectrophotometry to Fatty Acid Derivatives," J. Am. Oil Chemists' Soc. 33, 1 (1956). F. L. Kauffman, "Infrared Spectroscopy of fat and Oils," J. Am. Oil Chemists' Soc. 41,4 (1964). W. J. Potts, Jr., Chemical Infrared Spectroscopy, Vol. I, innovations, Wiley, ny, 1963. R. S. Tipson, Infrared Spectroscopy of Carbohydrates, nationwide Bureau of criteria Monograph llO, Washington, D.C., 1968. C. N. R. Rao, Chemical functions of Infrared Spectroscopy, educational Press, manhattan, 1963.
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Additional resources for Applications of Infrared Spectroscopy in Biochemistry, Biology, and Medicine
1-mm cell. 3 (Continued) cm- 1 Compound or structural group 730 Polyethylene 727 Na 2 SiF 6 719 697 Polyethylene Polystyrene 667 CO 2 Band position, Comments Polyethylene now is so widely used for making all kinds of laboratory ware that it appears occasionally as a contaminant in samples. Polyethylene has a strong doublet with components at 730 and 719cm-'. Silicon tetrafluoride attacks a sodium chloride window forming sodium silicofluoride. See 730 cm -, band. Polystyrene vials, used for mixing solid samples with KBr on mechanical vibrators, are easily abraded.
A. J. Am. Chem. Soc. 86, 4774 (1964). Kotani, M. in Advances in Chemical Physics, Vol. 7: The Structure and Properties of Biomolecules and Biological Systems (J. ), Interscience, New York, 1964, p. 159. McCabe, W. C. and Fisher, H. F. Nature 207, 1274 (1965). McCallum, J. D. in Progress in Infrared Spectroscopy, Vol. 2 (H. A. ) Plenum Press, New York, 1964, p. 227. , and Fujioka, O. 1. Am. Chem. Soc. 72, 3490 (1950). Murthy, A. S. N. and Rao, C. N. R. "Hydrogen Bonding," Tech. Report No. I of the Department of Chemistry, Indian Institute of Technology, Kanpur, India, 1964.
1-Mono- and 2-monoglycerides can be quantitated by plots of absorbances of the 6993 cm - 1 band versus concentration. The C-H stretching bands of 1,2- and 1,3-diglycerides have been investigated and the spectra of these isomers showed possibilities of three main configurations (Kauffman, 1964), one internally hydrogen-bonded, and two with no hydrogen bond involvement. The fraction of hydrogen-bonded molecules seemed to be relatively low. The hydrogen-bonded form of 1,3-diglycerides was believed to have a trans-gauche configuration around the glyceride C-C bond, and the non-hydrogen-bonded forms to have probably a trans-trans configuration around the glyceride backbone, OH being either trans or gauche with respect to the nearest C-H group.